Bond Strength of a Novel One Bottle Multi-mode Adhesive to Human Dentin After
Six Months of Storage
Fernanda Borguetti Manfroi1, Maurem Leitão Marcondes1, Deise Caren Somacal1, Gilberto Antonio Borges2, Luiz Henrique Burnett Júnior1, Ana Maria Spohr3, *
1 Department of Restorative Dentistry, School of Dentistry, Pontifical Catholic University of Rio Grande do Sul, Porto Alegre, Brazil
2 Department of Restorative Dentistry, Uberaba University, Uberaba, Brazil
3 Department of Dental Materials, School of Dentistry, Pontifical Catholic University of Rio Grande do Sul, Porto Alegre, Brazil
The aim of the study was to evaluate the microtensile bond strength (µTBS) of Scotchbond Universal to dentin using the etch-and-rinse or the self-etch technique after 24 h and 6 months of storage.
Materials and Methods:
Flat dentin surfaces were obtained in 24 third molars. The teeth were divided into four groups: G1 – Scotchbond Universal applied in the etch-and-rinse mode; G2 – Scotchbond Universal applied in the self-etch mode; G3 – Scotchbond Multi-Purpose; G4 – Clearfil SE Bond. A block of composite was built on the adhesive area. The tooth/resin sets were cut parallel to the long axis to obtain 40 beams (~0.8 mm2) for each group. Twenty specimens were immediately submitted to the µTBS test, and the remaining 20 were stored in water for 6 months. Failures and the adhesive interface were analyzed by SEM.
According to two-way ANOVA, the interaction between adhesive and storage time was significant (p=0.015).The µTBS (MPa) means were the following: 24 h – G1 (39.37±10.82), G2 (31.02±13.76), G3 (35.09±14.03) and G4 (35.84±11.06); 6 months – G1 (36.99±8.78), G2 (40.58±8.07), G3 (32.44±6.07) and G4 (41.75±8.25). Most failures were mixed. Evidence of hybrid layer and numerous resin tags were noted for Scotchbond Universal applied with the etch-and-rinse mode and Scotchbond Multi-Purpose. A thinner hybrid layer and fewer resin tags were noted for Scotchbond Universal applied in the self-etch mode and Clearfil SE Bond.
The results indicate that the µTBS for Scotchbond Universal is comparable to the gold-standard adhesives. Scotchbond Universal applied in the self-etch mode and Clearfil SE Bond revealed higher bond stability compared to the etch-and-rinse mode.
Keywords: Adhesive systems, Bond strength, Dentin, Interface, Microtensile, Storage.
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* Address correspondence to this author at the School of Dentistry – Pontifical Catholic University of Rio Grande do Sul,
Avenida Ipiranga, 6681
90616-900 Porto Alegre, RS, Brazil; Tel/Fax: +55-51-33203538; E-mail: email@example.com