Table 6: Selected bond lengths (Å) and angles(°) for cyCuKNi.
Bond lengths
|
|
|
|
Cu1-N1
|
1.934(7)
|
Cu2-N3
|
1.907(8)
|
Cu1-N2
|
1.989(8)
|
Cu2-N4
|
1.964(7)
|
Cu1-O2
|
1.885(7)
|
Cu2-O6
|
1.915(6)
|
Cu1-O4
|
1.927(6)
|
Cu2-O8
|
1.941(7)
|
Cu1-N5
|
2.435(8)
|
Cu2-N6
|
2.403(9)
|
Ni1-C45
|
1.822(12)
|
Ni1-C47
|
1.861(11)
|
Ni1-C46
|
1.912(11)
|
Ni1-C48
|
1.861(10)
|
K1-O1
|
2.716(7)
|
K2-O5
|
2.771(7)
|
K1-O2
|
2.696(7)
|
K2-O6
|
2.723(7)
|
K1-O3
|
2.765(7)
|
K2-O7
|
2.727(7)
|
K1-O4
|
2.705(7)
|
K2-O8
|
2.707(7)
|
K1-N6#2
|
2.864(9)
|
K2-N5#1
|
2.868(10)
|
|
|
K2-N8#1
|
3.170(11)
|
Bond angles
|
|
|
|
N1-Cu1-N2
|
83.5(3)
|
N3-Cu2-N4
|
85.5(3)
|
N1-Cu1-O2
|
94.3(3)
|
N3-Cu2-O6
|
94.5(3)
|
N1-Cu1-O4
|
173.9(3)
|
N3-Cu2-O8
|
172.5(3)
|
N2-Cu1-O2
|
169.3(3)
|
N4-Cu2-O6
|
166.2(3)
|
N2-Cu1-O4
|
92.6(3)
|
N4-Cu2-O8
|
92.0(3)
|
O2-Cu1-O4
|
88.6(3)
|
O6-Cu2-O8
|
86.3(3)
|
C45-Ni1-C46
|
178.0(6)
|
C46-Ni1-C47
|
86.1(4)
|
C45-Ni1-C47
|
94.3(4)
|
C46-Ni1-C48
|
91.2(4)
|
C45-Ni1-C48
|
88.5(5)
|
C47-Ni1-C48
|
176.1(6)
|
O1-K1-O2
|
57.3(2)
|
O5-K2-O6
|
56.5(2)
|
O1-K1-O3
|
172.7(2)
|
O5-K2-O7
|
164.2(2)
|
O1-K1-O4
|
116.4(2)
|
O5-K2-O8
|
114.4(2)
|
O2-K1-O3
|
115.5(2)
|
O6-K2-O7
|
114.4(2)
|
O2-K1-O4
|
59.06(19)
|
O6-K2-O8
|
58.13(19)
|
O3-K1-O4
|
56.6(2)
|
O7-K2-O8
|
56.9(2)
|
Symmetry operation:
#1 [x, y, -1+z],
#2 [x, y, 1+z].