| No | Compound | Color | Yield (%) |
M.Wt | D.T/0C | Analysis Calc. (F)% | (Λm)a | ||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| C | H | N | M | X | |||||||
| 1 | [FeLCl2].½EtOH.½H2O | Black | 93 | 680.8 | 300 | 61.69(61.91) | 4.4(4.51) | 8.22(8.32) | 8.19(7.44) | 10.43(9.94) | 23 |
| 2 | [CoLCl(OH)].H2O | Black | 63 | 651.4 | 322 | 62.63 (62.06) | 4.2 (3.53) | 8.59(9.05) | 9.04(8.83) | 10.89(10.65) | 16 |
| 3 | [CoLNO3(OH)].1½H2O | Black | 90 | 678.9 | 200 | 60.09 (59.24) | 4.42 (3.51 ) | 10.31(10.37) | 8.67(8.84) | - | 31 |
| 4 | [CoL(OAc)OH].½EtOH | Black | 100 | 698.9 | 230 | 65.24(66.56) | 4.57 (4.37) | 8.01 (8.2) | 8.16(8.25) | - | 2 |
| 5 | [NiLCl.H2O]Cl.H2O.½EtOH | Black | 83 | 710.7 | 340 | 59.09 (60.03) | 4.64 (3.72) | 7. 88(8.39) | 8.47(7.82) | 10.25(10.65) | 66 |
| 6 | [NiL(OAc)OH].½EtOH | Black | 95 | 679.7 | 280 | 65.32 (65.69) | 4.85 (4.44) | 8.24 (8.16) | 8.64(8.8) | - | 16 |
| 7 | [CuLCl2].2H2O | Black | 100 | 692.5 | 300 | 58.92 (59.68) | 4.33(3.97) | 8.08(8.02) | 9.16(8.47) | 10.25(9.47) | 29 |
| 8 | [CuLBr(OH)].½EtOH | Black | 100 | 705.5 | 230 | 59.53(60.79) | 4.25 (3.31) | 7.94 (7.51) | 11.26(11.5) | 11.34(10.91) | 35 |
| 9 | [CuL(OH)]NO3.H2O | Black | 92 | 683.5 | 154 | 59.69(60.03) | 4.24(4.12) | 8.19 (8.94) | 9.29(8.89) | - | 62 |
|
10 |
[CuL(OH)H2O]ClO4.½EtOH |
Black |
100 | 716.5 |
- |
59.8(60.85) | 4.33(4.06) |
7. 76(7.65) |
9.4(10.58) |
13.79(13.93) | 63 |
| 11 | [PdLCl.H2O]Cl.2½H2O | Black |
100 |
762.4 | 220 |
53.51(54.48) |
4.33(4.04) | 7.34(7.75) | 13.95(14.18) |
9.31(9.46) |
66 |