| Chemical formula: C130H134Cu2N6O26 |
| Formula weight = 2323.57 |
| T = 100 K |
| Crystal system: triclinic Space group: P |
| a = 10.430(3) Å α = 109.406(4)° |
| b = 15.847(5) Å β = 92.717(4)° |
| c = 19.990(6) Å γ = 108.669(4)° |
| V = 2908.3(16) Å3Z = 1 |
| Dx = 1.327 g/cm3 |
| Radiation: Mo Kα (λ = 0.71073 Å) |
| µ(Mo Kα) = 0.444 mm–1F(000) = 1222 |
| Crystal size = 0.12 x 0.08 x 0.03 mm3 |
| No. of reflections collected = 13796 |
| No. of independent reflections = 9988 |
| θ range for data collection: 1.10 to 25.02° |
| Data/Restraints/Parameters = 9988/0/745 |
| Goodness-of-fit on F2 = 0.985 |
| R indices [I>2σ(I)]: R1 = 0.0673, wR2 = 0.1605 |
| R indices (all data): R1 = 0.0949, wR2 = 0.1770 |
| (Δ/σ)max = 0.000 |
| (Δρ)max = 1.087 eÅ–3 (Δρ)min = –0.642 eÅ–3 |
| Measurement: Bruker Smart APEX-II ULTRA diffractometer |
| Program system: SHELXTL |
| Structure determination: Direct methods (SHELXS-97) |
| Refinement: full matrix least-squares (SHELXL-97) |
| CCDC deposition number: 1815964 |