|
100 K |
150 K |
200 K |
250 K |
294 [32] |
< C10F8(plane)a axis |
66.5(4) |
66.6(4) |
66.5(4) |
66.6(4) |
66.7 |
< C10H8(plane)a axis |
70.3(4) |
70.2(4) |
70.2(4) |
70.1(4) |
69.9 |
< C10F8(plane)bc plane |
30.05(4) |
30.03(5) |
30.2(1) |
30.2(1) |
30.5 |
< C10H8(plane)bc plane |
25.85(6) |
26.0(1) |
26.2(1) |
26.4(1) |
26.7 |
< C10F8(plane) C10F8(plane)b
|
33.51(8) |
33.63(7) |
33.9(1) |
34.1(1) |
34.1 |
< C10H8(plane) C10H8(plane)b
|
30.54(6) |
30.7(1) |
30.9(1) |
31.2(1) |
31.5 |
C10F8(plane)···C10F8(plane)
|
6.704(3) |
6.743(3) |
6.771(3) |
6.813(3) |
6.847 |
offset C10F8···C10F8
|
2.919(3) |
2.922(3) |
2.941(3) |
2.949(3) |
2.954 |
C10H8(plane)···C10H8(plane)
|
6.885(3) |
6.916(3) |
6.947(3) |
6.979(3) |
7.004 |
Offset C10H8···C10H8
|
2.462(3) |
2.485(3) |
2.497(3) |
2.529(3) |
2.559 |
˂ C10F8(plane) C10H8(plane)
|
4.30(8) |
4.08(6) |
4.1(1) |
3.9(1) |
3.7 |
C10H8(centre)···C10F8(centre)
|
3.656(3) |
3.675(3) |
3.691(3) |
3.711(3) |
3.728 |
C10H8(centre)···C10F8(plane)
|
3.352(3) |
3.372(3) |
3.385(3) |
3.407(3) |
3.424 |
offset |
1.460(3) |
1.461(3) |
1.471(3) |
1.471(3) |
1.475 |
C10F8(centre)···C10H8(plane)
|
3.442(3) |
3.458(3) |
3.473(3) |
3.490(3) |
3.502 |
offset |
1.232(3) |
1.244(3) |
1.250(3) |
1.262(3) |
1.278 |
C(13)···F(4) |
3.258(2) |
3.282(2) |
3.309(3) |
3.334(3) |
3.360 |
C(14)···F(3) |
3.587(2) |
3.602(2) |
3.629(2) |
3.648(2) |
3.681 |
F(3)···F(4) |
3.053(2) |
3.067(2) |
3.081(2) |
3.097(2) |
3.114 |
F(4)···F(4) |
2.757(2) |
2.776(2) |
2.801(2) |
2.828(2) |
2.865 |
C(14)···C(14) |
3.852(3) |
3.876(3) |
3.909(3) |
3.941(3) |
3.987 |
C(13)···C(14) |
4.124(2) |
4.144(2) |
4.168(3) |
4.193(3) |
4.225 |
C(12)···F(5) |
3.326(2) |
3.349(2) |
3.370(3) |
3.393(3) |
3.410 |
C(13)···F(5) |
3.260(2) |
3.281(2) |
3.310(3) |
3.331(3) |
3.360 |
C(13)···F(2) |
3.725(2) |
3.751(2) |
3.784(3) |
3.813(3) |
3.856 |
F(2)···F(4) |
2.792(2) |
2.814(2) |
2.832(2) |
2.857(2) |
2.891 |
F(5)···F(4) |
2.988(2) |
3.005(2) |
3.024(2) |
3.050(2) |
3.079 |
F(3)···F(5) |
3.292(2) |
3.321(2) |
3.347(2) |
3.382(2) |
3.420 |